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- W4366463586 abstract "This study reports a carbonylative acetylation for the synthesis of N-phenyl-N-(pyridin-2-yl)acetamides using N,N-dimethylformamide (DMF) as a methyl source and CO as a carbonyl source. Interestingly, dimethyl sulfoxide (DMSO) can be also used as a methyl source when using only DMSO as the solvent. Mechanistic studies using DMSO-d6 revealed that the methyl group was derived from the methyl group of DMF instead of DMSO when using DMF and DMSO as a mixed solvent. These results indicated that DMF was a preferential methyl source." @default.
- W4366463586 created "2023-04-22" @default.
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- W4366463586 date "2023-04-20" @default.
- W4366463586 modified "2023-10-13" @default.
- W4366463586 title "A Palladium-Catalyzed Carbonylative Acetylation of <i>N</i>-Phenylpyridin-2-amine Using DMF and CO as the Acetyl Source" @default.
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- W4366463586 doi "https://doi.org/10.1021/acs.joc.3c00176" @default.
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