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- W4366985308 abstract "Synthesis of unusual phenanthroporphyrins was achieved by a stepwise precursor method. Precursor porphyrins fused with aryl-substituted bicyclo[2.2.2]octadiene afforded the corresponding arylbenzoporphyrins (arylBPs) by a retro Diels-Alder reaction. Unusual phenanthroporphyrins were obtained via the intramolecular Scholl reaction of arylBPs. X-ray crystallographic analysis revealed a distorted, helical porphyrin plane. Red-shifted absorptions of tetraphenanthroporphyrin are observed at ca. 580 nm for the B band and at 700-900 nm for the Q bands. Analysis of magnetic circular dichroism spectra and time-dependent density functional theory calculations was used to explain the optical properties and electronic structures." @default.
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- W4366985308 date "2023-04-25" @default.
- W4366985308 modified "2023-10-15" @default.
- W4366985308 title "Synthesis of Peripherally Annulated Phenanthroporphyrins" @default.
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- W4366985308 doi "https://doi.org/10.1021/acs.orglett.3c00876" @default.
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