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- W4366998291 abstract "Abstract A set of Pd nanoclusters embedded in rGO, referred to as Pd@rGO ( viz. Pd@rGO 0.16 , Pd@rGO 0.32, Pd@rGO 0.48, Pd@rGO 1 ), where subscripts indicate the mmol of cetyltrimethylammonium bromide (CTAB) were synthesized using water as a solvent by simply varying the amount of CTAB that was used to control both morphology and size. TEM analysis indicated that the average particle sizes of Pd@rGO 0.16 and Pd@rGO 0.32 fall in the range of 4.5-5.0 nm and 20–25 nm, respectively. On the other hand, particles were found to be agglomerated in Pd@rGO 0.48 and Pd@rGO 1 . The Pd@rGO 0.16 composite was exhaustively characterized by TEM, SEM-EDAX, powder X-ray diffraction, XPS, and ICP-AES measurements. ICP-AES analysis of Pd@rGO 0.16 indicated that 0.01g of Pd@rGO 0.16 contains 0.09 mol % Pd. The catalytic potentiality of these NPs was investigated for direct C(sp 2 )-H bond activation of various indoles with aryl boronic acids. Among the four composites, Pd@rGO 0.16 exhibited the best activity for the abovementioned organic transformation. Different indoles with varying electronic groups underwent coupling with aryl boronic acids giving up to 86% product yield. It was retrievable for up to five consecutive catalytic cycles without compromising its catalytic activity." @default.
- W4366998291 created "2023-04-27" @default.
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- W4366998291 date "2023-04-25" @default.
- W4366998291 modified "2023-09-25" @default.
- W4366998291 title "CTAB-assisted synthesis of reduced graphene oxide supported Pd nanoparticles(Pd@rGO) as a sustainable heterogeneous catalyst for C-2 arylation of indoles with arylboronic acids." @default.
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- W4366998291 doi "https://doi.org/10.21203/rs.3.rs-2711303/v1" @default.
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