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- W4367675062 abstract "A new analytical method to identify sulfur mustard (HD) using liquid chromatography-electrospray ionization-tandem mass spectrometry (LC‒ESI‒MS/MS) after derivatization with diethanolamine was developed. The method has been successfully applied to identify HD spiked into both soil and asphalt extracts containing diesel, which resembles a diesel exhaust environment that may be encountered in battlefield conditions or in terror attacks. The LC-ESI-MS/MS method enables the sensitivity enhancement compared with conventional GC-EI-MS analysis and in addition, identifies HD in a complex hydrocarbon matrix. The calibration curve for the derivatization product was linear in the range of 50–5000 pg/mL with correlation coefficients (R2) greater than 0.99 and a LOI of 50 pg/mL. The recoveries (n = 3) were observed at >90% with soil and asphalt containing ∼10 mg/ml diesel. Thus, this method provides a robust evidence of HD use." @default.
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- W4367675062 date "2023-08-01" @default.
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- W4367675062 title "Identification of sulfur mustard in complex environmental samples based on derivatization and LC-ESI-MS/MS analysis" @default.
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- W4367675062 doi "https://doi.org/10.1016/j.ijms.2023.117066" @default.
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