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- W4367676035 abstract "A general and broadly applicable cobalt-catalyzed multicomponent 1,2-perfluoroalkylation carbonylation of alkenes has been developed. This protocol allows the synthesis of β-perfluoroalkyl-substituted amides, esters, and related derivatives using olefins, carbon monoxide, commercially accessible perfluoroalkyl iodides, and a variety of nucleophiles including low nucleophilic amides and urea derivatives in a one-pot manner. As an example, readily available trifluoroiodomethane can be utilized forming pharmaceutically relevant β-trifluoromethylated amides. To showcase the application potential, the perfluoroalkylation carbonylation process was applied to selected current drugs and biologically active molecules. The methodology permits a straightforward increase of the molecular complexity of olefins toward functionalized perfluoroalkylated building blocks in a regioselective manner." @default.
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- W4367676035 date "2023-05-02" @default.
- W4367676035 modified "2023-10-04" @default.
- W4367676035 title "Cobalt-Catalyzed Multicomponent Carbonylation of Olefins: Efficient Synthesis of β-Perfluoroalkyl Imides, Amides, and Esters" @default.
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- W4367676035 doi "https://doi.org/10.1021/acscatal.3c00771" @default.
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