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• W4367843410 abstract "A scalable and chromatography-free synthesis of enantiopure N-Boc-trans-4-methyl-l-prolinol (1) on the multi-gram scale is described. Two shortest possible routes have been developed using commercially available and inexpensive amino acids such as 4-hydroxy-l-proline and l-pyroglutamic acid to afford 1 (>99% purity by high-performance liquid chromatography) with a moderate yield. This chiral precursor can act as a promising building block by providing practical access to a diverse array of 4-alkyl-l-prolines." @default.
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• W4367843410 date "2023-05-03" @default.
• W4367843410 modified "2023-09-23" @default.
• W4367843410 title "Short and Scalable Synthesis of Enantiopure <i>N</i>-Boc-<i>trans</i>-4-methyl-<scp>L</scp>-prolinol" @default.
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• W4367843410 doi "https://doi.org/10.1021/acs.oprd.3c00053" @default.
• W4367843410 hasPublicationYear "2023" @default.
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