Matches in SemOpenAlex for { <https://semopenalex.org/work/W4376113242> ?p ?o ?g. }
Showing items 1 to 90 of
90
with 100 items per page.
- W4376113242 endingPage "105388" @default.
- W4376113242 startingPage "105388" @default.
- W4376113242 abstract "A molecularly imprinted polymer (MIP) was synthesized and assessed as a selective extraction phase in the microextraction by packed sorbent (MEPS) of sulfonylureas herbicides (SUHs) — Thifensulfuron, Chlorosulfuron, Tribenuron, and Bensulfuron — from grounded corn samples. Bensulfuron was employed as the template for the MIP preparation. MIP particles were chemically and structurally characterized. Distribution (Kd), selectivity (k), and relative selectivity (k') coefficients were estimated using binary mixtures of bensulfuron/betazon and bensulfuron/prometon. The most significant parameters affecting the MEPS performance were systematically studied in univariate and multivariate experiments. Analyses were performed by liquid chromatography coupled to time-of-flight mass spectrometry (LC-ToF). Under selected conditions, the developed MIP-MEPS-LC-ToF method demonstrated suitable analytical confidence and reliability. Determination coefficients (r2) higher than 0.9940, and limits of detection (LODs) of 2.5 µg kg-1 were obtained. Intra- and interday precision was lower than 14.2%, and accuracy ranged between 89.6% and 113.6%. The synthesized MIP demonstrated enhanced selectivity and higher SUHs uptake capability compared to the non-imprinted polymer (NIP) and tested commercial sorbents. Besides, the method is a cheap, feasible, and environmentally friendly analytical tool. A single MEPS device packed with 1.0 mg of MIP was reused more than 180 times without loss in its extraction capabilities." @default.
- W4376113242 created "2023-05-12" @default.
- W4376113242 creator A5021859427 @default.
- W4376113242 creator A5043604785 @default.
- W4376113242 creator A5087057938 @default.
- W4376113242 creator A5091703919 @default.
- W4376113242 date "2023-08-01" @default.
- W4376113242 modified "2023-10-16" @default.
- W4376113242 title "A molecularly imprinted polymer for microextraction by packed sorbent of sulfonylureas herbicides from corn samples" @default.
- W4376113242 cites W1994769873 @default.
- W4376113242 cites W2020282250 @default.
- W4376113242 cites W2021518132 @default.
- W4376113242 cites W2034038607 @default.
- W4376113242 cites W2046496054 @default.
- W4376113242 cites W2050226999 @default.
- W4376113242 cites W2059245754 @default.
- W4376113242 cites W2062049317 @default.
- W4376113242 cites W2096100182 @default.
- W4376113242 cites W2110311424 @default.
- W4376113242 cites W2133571744 @default.
- W4376113242 cites W2143536105 @default.
- W4376113242 cites W2227404551 @default.
- W4376113242 cites W2943219301 @default.
- W4376113242 cites W2947896354 @default.
- W4376113242 cites W3028107617 @default.
- W4376113242 cites W3155585193 @default.
- W4376113242 cites W4214498199 @default.
- W4376113242 cites W4229007835 @default.
- W4376113242 cites W4283323630 @default.
- W4376113242 cites W4284970685 @default.
- W4376113242 cites W4292489487 @default.
- W4376113242 cites W4376596242 @default.
- W4376113242 cites W862087197 @default.
- W4376113242 cites W3149483073 @default.
- W4376113242 doi "https://doi.org/10.1016/j.jfca.2023.105388" @default.
- W4376113242 hasPublicationYear "2023" @default.
- W4376113242 type Work @default.
- W4376113242 citedByCount "1" @default.
- W4376113242 countsByYear W43761132422023 @default.
- W4376113242 crossrefType "journal-article" @default.
- W4376113242 hasAuthorship W4376113242A5021859427 @default.
- W4376113242 hasAuthorship W4376113242A5043604785 @default.
- W4376113242 hasAuthorship W4376113242A5087057938 @default.
- W4376113242 hasAuthorship W4376113242A5091703919 @default.
- W4376113242 hasConcept C118792377 @default.
- W4376113242 hasConcept C119128265 @default.
- W4376113242 hasConcept C150394285 @default.
- W4376113242 hasConcept C161790260 @default.
- W4376113242 hasConcept C162356407 @default.
- W4376113242 hasConcept C162602672 @default.
- W4376113242 hasConcept C178790620 @default.
- W4376113242 hasConcept C185592680 @default.
- W4376113242 hasConcept C2777899863 @default.
- W4376113242 hasConcept C43617362 @default.
- W4376113242 hasConcept C4725764 @default.
- W4376113242 hasConcept C81426234 @default.
- W4376113242 hasConceptScore W4376113242C118792377 @default.
- W4376113242 hasConceptScore W4376113242C119128265 @default.
- W4376113242 hasConceptScore W4376113242C150394285 @default.
- W4376113242 hasConceptScore W4376113242C161790260 @default.
- W4376113242 hasConceptScore W4376113242C162356407 @default.
- W4376113242 hasConceptScore W4376113242C162602672 @default.
- W4376113242 hasConceptScore W4376113242C178790620 @default.
- W4376113242 hasConceptScore W4376113242C185592680 @default.
- W4376113242 hasConceptScore W4376113242C2777899863 @default.
- W4376113242 hasConceptScore W4376113242C43617362 @default.
- W4376113242 hasConceptScore W4376113242C4725764 @default.
- W4376113242 hasConceptScore W4376113242C81426234 @default.
- W4376113242 hasFunder F4320320997 @default.
- W4376113242 hasFunder F4320321091 @default.
- W4376113242 hasFunder F4320322025 @default.
- W4376113242 hasLocation W43761132421 @default.
- W4376113242 hasOpenAccess W4376113242 @default.
- W4376113242 hasPrimaryLocation W43761132421 @default.
- W4376113242 hasRelatedWork W1979301814 @default.
- W4376113242 hasRelatedWork W1996131936 @default.
- W4376113242 hasRelatedWork W2032719152 @default.
- W4376113242 hasRelatedWork W2170176786 @default.
- W4376113242 hasRelatedWork W2672832028 @default.
- W4376113242 hasRelatedWork W2787917012 @default.
- W4376113242 hasRelatedWork W3083689796 @default.
- W4376113242 hasRelatedWork W3216112257 @default.
- W4376113242 hasRelatedWork W4200138122 @default.
- W4376113242 hasRelatedWork W4386303499 @default.
- W4376113242 hasVolume "121" @default.
- W4376113242 isParatext "false" @default.
- W4376113242 isRetracted "false" @default.
- W4376113242 workType "article" @default.