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• W4377966286 abstract "Electrolytic reduction technology plays a significant role in industrial metal production. In present work, cyclic voltammetry (CV) and square wave voltammetry (SWV) were applied to study the electrochemical behaviors of ZnO cathode in the CaCl 2 -NaCl melt at 873 K. During the experiment, we found that the dissolution-electrodeposition mechanism (ZnO = Zn 2+ + O 2− , Zn 2+ + 2e − = Zn) dominates the electrolytic reduction of ZnO, and the contribution of the direct-reduction from solid phase (ZnO + 2e − = Zn + O 2− ) is small. Furthermore, the electro-reduction of ZnO was conducted by potentiostatic electrolysis. The peak potential of ZnO to Zn was −0.48 V vs Ag/Ag + . Therefore, the metallic Zn can be obtained at an applied potential of −0.80 V (vs Ag/Ag + ). When the applied potential increased to −2.00 V (vs Ag/Ag + ), the Zn and CaZn 3 alloy were formed simultaneously. The electrolytic products were confirmed by X-ray diffraction (XRD) analysis. This study proved the feasibility of electro-reduction technology to prepare Zn metal through the reduction of ZnO material." @default.
• W4377966286 created "2023-05-25" @default.
• W4377966286 creator A5034397565 @default.
• W4377966286 creator A5055131988 @default.
• W4377966286 date "2023-06-01" @default.
• W4377966286 modified "2023-09-25" @default.
• W4377966286 title "Electrolytic Reduction of ZnO in the CaCl₂-NaCl Molten Salt" @default.
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• W4377966286 doi "https://doi.org/10.1149/1945-7111/acd87f" @default.
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