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- W4378619281 abstract "Analysis of the data in the Cambridge Structural Database (CSD) for compounds containing an {M(tpy)X3} motif (tpy = 2,2’:6’,2”-terpyridine, M = any metal, X = F, Cl, Br, I) reveals 17 isostructural mononuclear [M(tpy)X3] compounds crystallizing without lattice solvent; both face-to-face π-stacking of pyridine rings and C–H3/H3’…X hydrogen bonding appear to be equally important. Regardless of coordination number (CN = 6, 7 or 8) and nuclearity (mono- or dinuclear), a recurring packing feature in other compounds containing an {M(tpy)X3} unit is the presence of bifurcated Cl…H3/H3’ interactions, complemented in some cases by Cl…H5’/H3” interactions, consistent with the acidic H3, H3’, H5’, and H3” atoms of a coordinated tpy ligand. Octahedral [M(tpy)F3] complexes crystallize as hydrates with strong F…H–OH hydrogen bonding dominating the crystal packing." @default.
- W4378619281 created "2023-05-29" @default.
- W4378619281 creator A5057669589 @default.
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- W4378619281 date "2023-05-28" @default.
- W4378619281 modified "2023-10-18" @default.
- W4378619281 title "C–H…X (X = F, Cl, Br, I) Versus π-Stacking in the Crystal Packing of Compounds Containing the {M(tpy)X3} Motif" @default.
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- W4378619281 doi "https://doi.org/10.3390/cryst13060885" @default.
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