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• W4379508734 abstract "Stable metal nitrides (MN) are promising materials to fit the future “green” ammonia–hydrogen nexus. Either through catalysis or chemical looping, the reductive hydrogenation of MN to MN1–x is a necessary step to generate ammonia. However, encumbered by the formation of kinetically stable M-NH1─3 surface species, this reduction step remains challenging under mild conditions. Herein, we discovered that deleterious Ti-NH1─3 accumulation on TiN can be circumvented photochemically with supported single atoms and clusters of platinum (Pt1-Ptn) under N2–H2 conditions. The photochemistry of TiN selectively promoted Ti-NH formation, while Pt1-Ptn effectively transformed any formed Ti-NH into free ammonia. The generated ammonia was found to originate mainly from TiN reduction with a minor contribution from N2 activation. The knowledge accrued from this fundamental study could serve as a springboard for the development of MN materials for more efficient ammonia production to potentially disrupt the century-old fossil-powered Haber–Bosch process." @default.
• W4379508734 created "2023-06-07" @default.
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• W4379508734 date "2023-06-06" @default.
• W4379508734 modified "2023-10-15" @default.
• W4379508734 title "Photochemical Acceleration of Ammonia Production by Pt₁-Pt<i>_n</i>-TiN Reduction and N₂ Activation" @default.
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• W4379508734 doi "https://doi.org/10.1021/jacs.3c01947" @default.
• W4379508734 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/37278596" @default.
• W4379508734 hasPublicationYear "2023" @default.
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