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- W4379801323 abstract "A divergent two-step process has provided access to optically pure enantiomers of MDMA and MDA, clinically relevant phenylisopropylamine entactogens. Target compounds were synthesized from commercially available alanine-derived aziridines. Critical process parameters were identified, and the reactions were optimized to avoid chromatographic purifications toward gram-scale isolations, providing (R)-(-)-MDMA, (S)-(+)-MDMA, (R)-(-)-MDA, and (S)-(+)-MDA each in greater than 98% purity by UPLC, >99% enantiomeric excess, and net yields between 50 and 60% for the complete process." @default.
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- W4379801323 date "2023-06-06" @default.
- W4379801323 modified "2023-09-25" @default.
- W4379801323 title "Swim in the Chiral Pool: MDMA and MDA Enantiomers from Alanine-Derived Precursors" @default.
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- W4379801323 doi "https://doi.org/10.1021/acsomega.3c02358" @default.
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