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- W4380182893 abstract "This study examines the differences in using two primary methods for adsorbing TMPO onto acid catalysts and their influence on the NMR spectra of TMPO-loaded zeolites. The findings show that TMPO molecules interact with both Brønsted and Lewis acid sites, and that the amount of (TMPO)2H+ dimers formed increases with the amount of TMPO added. The use of dichloromethane as a solvent inhibits the formation of dimers and crystalline TMPO but may lead to inaccurate estimations of acid site strength and quantification due to interactions with residual solvent molecules. The gas-phase method is preferred for adsorbing TMPO onto zeolites, but caution is needed to avoid forming a high number of dimers that make interpretation of the NMR spectra challenging." @default.
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- W4380182893 date "2023-10-01" @default.
- W4380182893 modified "2023-10-03" @default.
- W4380182893 title "Investigating trimethylphosphine oxide interactions with Brønsted and Lewis acid sites in zeolites: A comparative solid-state NMR study of wet-phase and gas-phase adsorption techniques" @default.
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- W4380182893 doi "https://doi.org/10.1016/j.micromeso.2023.112666" @default.
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