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- W4380291946 abstract "We developed one-flow syntheses of unsymmetrical sulfamides and N-substituted sulfamate esters by changing a nucleophile and a tertiary amine from inexpensive and commercially available chlorosulfonic acid. In the synthesis of N-substituted sulfamate esters, unexpected symmetrical sulfite formation was suppressed by changing the tertiary amine. The effect of tertiary amines was proposed using linear regression. Our approach rapidly (≤90 s) provides desired products containing acidic and/or basic labile groups without tedious purification under mild (20 °C) conditions." @default.
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- W4380291946 date "2023-06-12" @default.
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- W4380291946 title "One-Flow Syntheses of Unsymmetrical Sulfamides and <i>N</i>-Substituted Sulfamate Esters" @default.
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- W4380291946 doi "https://doi.org/10.1021/acs.orglett.3c01546" @default.
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