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• W4381470322 startingPage "8770" @default.
• W4381470322 abstract "Herein, we report a concise synthetic approach for the first total synthesis of a pentasaccharide repeating unit of Acinetobacter baumannii K11 capsular polysaccharides containing a rare sugar 6-deoxy-l-talose. The pentasaccharide was synthesized in a convergent manner using a [3 + 2] block glycosylation strategy. During this synthetic strive, we used a 2,2,2-trichloroethoxycarbonyl (Troc)-protected monosaccharide unit to achieve a high yield during the glycosylation to synthesize a trisaccharide, and chemoselective deprotection of the Troc group from the trisaccharide was carried out under a mild, pH-neutral condition, keeping the O-glycosidic bond, azido, and acid/base sensitive group intact. A thiotolylglycoside disaccharide donor containing 6-deoxy-l-talose was synthesized for the first time by the armed-disarmed glycosylation method between two thiotolylglycosides." @default.
• W4381470322 created "2023-06-22" @default.
• W4381470322 creator A5038988437 @default.
• W4381470322 creator A5046602857 @default.
• W4381470322 date "2023-06-21" @default.
• W4381470322 modified "2023-09-26" @default.
• W4381470322 title "Total Synthesis of 6-Deoxy-<scp>l</scp>-talose Containing a Pentasaccharide Repeating Unit of <i>Acinetobacter baumannii</i> K11 Capsular Polysaccharides" @default.
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• W4381470322 doi "https://doi.org/10.1021/acs.joc.3c00615" @default.
• W4381470322 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/37340701" @default.
• W4381470322 hasPublicationYear "2023" @default.
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