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- W4381569583 abstract "Holliday’s industrial dye synthesis of 1865 was repeated by heating aniline hydrochloride with nitrobenzene and the products were characterised by modern spectroscopic methods. A red dye was isolated in low yield and characterised by an X-ray single-crystal structure determination as 9-phenyl-3-anilinophenazone-2-anil. The structure was identical to that made 93 years later in 1958 by the oxidation of 2-aminodiphenylamine hydrochloride with FeCl 3 followed by heating the two products with aniline. An X-ray single-crystal structure determination was obtained for an isomer of anilinoaposafranine. A proposal is made that 9-phenyl-3-anilinophenazone-2-anil, isolated from Holliday’s synthesis, arises via the oxidation and dimerisation of 2-aminodiphenylamine with hot nitrobenzene so there is a common intermediate in both syntheses." @default.
- W4381569583 created "2023-06-22" @default.
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- W4381569583 date "2023-05-01" @default.
- W4381569583 modified "2023-09-24" @default.
- W4381569583 title "Uncovering John Holliday’s industrial dye synthesis patented in 1865" @default.
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- W4381569583 doi "https://doi.org/10.1177/17475198231175602" @default.
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