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- W4381852022 abstract "A rapid and simple magnetic solid phase extraction-liquid chromatography-tandem mass spectrometry method is reported to determine vancomycin in human plasma. The Fe3O4@SiO2 nanocomposite was prepared using silica nanoparticles obtained from rice husk waste and its modification using ammonia solution to obtain a Fe3O4@SiO2-NH2 nanohybrid as a new sorbent. The structure and morphology of the sorbent were characterized by X-ray diffraction, field emission scanning electron microscopy, and Fourier transform infrared spectroscopy. The nanosorbent was successfully used in magnetic solid phase extraction without hazardous solvents in 9 min with analysis by high-performance liquid chromatography – tandem mass spectrometry. Under the optimized conditions, the method provided a linear range from 10 to 1000 ng mL−1. The intra-day (n = 3) and inter-day precision (n = 3 working days) were below 10% relative standard deviation. The developed procedure was employed for determining vancomycin in human plasma with recoveries from 84.0 to 109.5% for spiked samples." @default.
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- W4381852022 date "2023-06-24" @default.
- W4381852022 modified "2023-09-27" @default.
- W4381852022 title "Determination of vancomycin in plasma with a magnetite amino silica adsorbent prepared from rice husks and high-performance liquid chromatography—tandem mass spectrometry (HPLC-MS/MS)" @default.
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- W4381852022 doi "https://doi.org/10.1080/10739149.2023.2221337" @default.
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