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• W4381888429 endingPage "105485" @default.
• W4381888429 startingPage "105485" @default.
• W4381888429 abstract "4-Mercaptobutyl glucosinolate (4-MBGSL) is a unique glucosinolate of rocket species (Diplotaxis, Eruca) in terms of having a free thiol group, rendering it capable of forming homo- and heteromeric disulfides. This oxidation process has been attributed to either incorrect sample preparation approaches or natural, stress-related events; accordingly, the conjugate of glutathione and 4-MBGSL could be regarded as an artefact. In our study, a set of experiments with UV-B irradiation was conducted on Eruca sativa plants to evaluate the formation of this conjugate. For validation purposes, the commercially unavailable conjugate of glutathione and 4-MBGSL was prepared through iodide assisted mild oxidation and characterized with high resolution mass spectrometry. The experiments revealed that UV-B-irradiation initiated the formation of not only this conjugate but a series of eight novel disulfide and polysulfide (up to four sulfur atoms linked) derivatives of 4-MBGSL, 1-thio-β-D-glucose, and glutathione metabolites, the structures of which were tentatively identified with MS/MS analysis. The natural formation of di- and polysulfides was also proven by ion mobility analysis to differentiate them from mass spectrometry (ion source) related artefact entities." @default.
• W4381888429 created "2023-06-25" @default.
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• W4381888429 date "2023-09-01" @default.
• W4381888429 modified "2023-10-09" @default.
• W4381888429 title "UV-B-radiation induced di- and polysulfide derivatives of 4-mercaptobutyl glucosinolate from Eruca sativa" @default.
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• W4381888429 doi "https://doi.org/10.1016/j.jfca.2023.105485" @default.
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