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- W4382021808 abstract "A novel chiral L-alanine-modified 3,4-ethylenedioxythiophene (EDOT) precursor, (2S)-(2,3-dihydrothieno[3,4-b][1,4]dioxin-2-yl)methyl 2-(tert-butoxy carbonylamino)propanoate (EDOT-Boc-Ala), was synthesized and electropolymerized in CH2Cl2–Bu4NBF. The corresponding polymer, poly((2S)-(2,3-dihydrothieno[3,4-b][1,4]dioxin-2-yl)methyl 2-(tert-butoxy carbonylamino)propanoate) (PEDOT-Boc-Ala) film showed good redox activity and stability. The electrochemical behavior, structural characterization, chirality, solubility, spectroscopic properties, thermal stability, and morphology of PEDOT-Boc-Ala film were investigated. Both doped and dedoped PEDOT-Boc-Ala film could well dissolve in strong polar solvents such as dimethyl sulfoxide, tetrahydrofuran, and acetone, etc. The determination of specific rotation showed that the electropolymerization of EDOT-Boc-Ala did not influence its conformation and the polymer exhibited an enhanced specific rotation ([α]20.0 = -191.08°) in comparison with that of the monomer ([α]20.0 = -30.77°). Moreover, the amperometric biosensor based on PEDOT-Boc-Ala film (as immobilization matrix of biologically-active species) was successfully fabricated and employed to determine the concentration of vitamin C." @default.
- W4382021808 created "2023-06-27" @default.
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- W4382021808 date "2013-02-01" @default.
- W4382021808 modified "2023-10-18" @default.
- W4382021808 title "Synthesis, Characterization, and Vitamin C Detection of a Novel L-Alanine-Modified PEDOT with Enhanced Chirality" @default.
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- W4382021808 doi "https://doi.org/10.1016/s1452-3981(23)14353-7" @default.
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