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• W4382022343 abstract "In this paper, the effect of electrodepositing current density on the composition, microstructure and electric properties of FeCo films were investigated in details by using EDS, XRD, SEM and XAS. The composition of Fe-Co films keeps nearly constant at different current densities. The deposited films have a mixed structure of fcc y phase and bcc a-Co7Fe3 phase. The bcc phase is dominant in the films electrodeposited at current density less than 40 mA/cm2 (<40 mA/cm2) while fcc phase is dominant in the film deposited at current density of 50 mA/cm2. High electrodepositing current density leads to a small decrease in the lattice parameter and an increase in grain sizes for the bcc phase. At all current densities, a colony-like morphology which consists of a lot of grain colonies having various sizes is seen. With increasing current densities (e.g., 10~20 mA/cm2), smooth, uniform and compact electrodeposits are obtained, while at higher current densities (e.g., 30~50 mA/cm2) the deposits are porous and cracks can be observed in the films. XAS results of the electrodeposited films indicate the presence of Fe3+ and Co2+ ions which mainly come from the surface oxidation of the as-deposited films and electrolytes." @default.
• W4382022343 created "2023-06-27" @default.
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• W4382022343 date "2013-01-01" @default.
• W4382022343 modified "2023-10-17" @default.
• W4382022343 title "XRD, SEM and XAS Studies of FeCo Films Electrodeposited at Different Current Density" @default.
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• W4382022343 doi "https://doi.org/10.1016/s1452-3981(23)14067-3" @default.
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