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- W4382022984 abstract "This work describes electrosynthesis of cadmium sulfide. A cadmium sulfide/cadmium nanocomposite in nanofibers form was synthesized by using, cadmium chloride (0.2 M), sodium thiosulfate (0.02 M) as precursor by the pulsed current of 100 mA cm-2 with a frequency of 8 Hz at solution temperature of 50°C. Cd content of the samples can be decreased by using of higher synthesis temperature. A pure nanostructured cadmium sulfide can be synthesized at temperature of 150°C. The morphology and particle size of each synthesized sample were studied by SEM, TEM and XRD. The cadmium sulfide nanopowder synthesized in the optimum conditions has excellent uniform nanofibers with a diameter range of 80 to 100 nm (average diameter of 90 nm) and length of 5μm to 7 μm. The obtained results indicate that the pulsed current electrochemical method can be used as a confident and controllable method for the preparation of cadmium sulfide nanofibers. Based on XRD studies, the samples were contaminated with cadmium impurity, which impurity was decreased by increasing of synthesis temperature. At solution temperature of 150°C (in electrohydrothermal bomb), cadmium sulfide was synthesized without any impurity of metallic cadmium." @default.
- W4382022984 created "2023-06-27" @default.
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- W4382022984 date "2010-05-01" @default.
- W4382022984 modified "2023-10-05" @default.
- W4382022984 title "Pulsed Current Electrochemical Synthesis of Cadmium Sulfide Nanofibers" @default.
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- W4382022984 doi "https://doi.org/10.1016/s1452-3981(23)15317-x" @default.
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