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• W4382023103 abstract "In this paper, cobalt nanorods were synthesized by the pulsed current electrochemical method on the stainless steel substrate in CoSO4 solution which its pH adjusted to 3 with adding sulfuric acid. In order to obatin uniform morphology, narrowest size distribution and best composition of sample, the effect of experimental variables such as concentration of cobalt ion, type and concentration of additive, pH, bath temperature, pulse frequency and pulse height (current amount), have been investigated. The composition, morphology and structure were investigated using Energy scanning electron microscopy (SEM), transmission electron microscopy (TEM) and X-ray diffraction techniques (XRD). The obtained results revealed that the optimized experimental conditions were 10 mA cm-2 current density, 8 Hz pulse frequency, 0.2 M Co2+, 0.4 M H3BO3, solution pH of 3, electrocrystallization temperature of 45 °C, 1.37 g/l PVP as structure director additive. The obtained results indicated that pulsed current electrochemical method can be used as a confident and controllable method for the preparation of the cobalt nanorods. The cobalt sample synthesized in the optimum conditions had uniform nanorods with average diameter of 35 nm and average length of 375 nm." @default.
• W4382023103 created "2023-06-27" @default.
• W4382023103 creator A5021728446 @default.
• W4382023103 creator A5049528116 @default.
• W4382023103 date "2010-07-01" @default.
• W4382023103 modified "2023-09-25" @default.
• W4382023103 title "Synthesis of Cobalt Nanorods by the Pulsed Current Electrochemical Method" @default.
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• W4382023103 doi "https://doi.org/10.1016/s1452-3981(23)15342-9" @default.
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