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- W4382364215 abstract "A low-cost, green catalyst for nitrobenzene (NB) hydrogenation is needed for aniline production. We report the preparation of highly-dispersed Co particles supported on N-doped carbons by the hydrothermal treatment of glucose, followed by the pyrolysis of a mixture of urea, glucose hydrochar and cobalt nitrate in one-pot. The effect of the pyrolysis temperature on the microstructure of the catalysts was studied. Results indicated that the activity for NB hydrogenation was highly affected by the surface area, Co-loading level and Co-Nx coordination in the catalysts. [email protected] pyrolyzed at 800 °C with 10% Co in the precursor had extraordinary activity for NB hydrogenation, achieving full conversion and 99% aniline selectivity in isopropanol at 100 °C and 1 MPa H2 pressure for 2.5 h. NB conversion and aniline selectivity over the catalysts remained almost unchanged after six recycles, due to the strong coordination between the N- and Co-species. The reaction system showed not only a high NB activity but also a green and durable catalytic process, with easy operation, easy separation and catalyst reusability." @default.
- W4382364215 created "2023-06-29" @default.
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- W4382364215 date "2023-06-01" @default.
- W4382364215 modified "2023-09-25" @default.
- W4382364215 title "Synthesis of Co―N―C catalysts from a glucose hydrochar and their efficient hydrogenation of nitrobenzene" @default.
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- W4382364215 doi "https://doi.org/10.1016/s1872-5805(23)60723-1" @default.
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