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- W4382583693 abstract "Wide use of phenylurea herbicide has caused serious residue problem and threaten human health. It is important to develop viable method for their sensitive determination. Herein, a multi-functionalized porous polymer was prepared by crosslinking hexafluorobisphenol A with pyromellitic dianhydride. Using the multi-functionalized porous polymer as solid phase extraction sorbent, combined with high performance liquid chromatography, a sensitive method was established for determining phenylurea herbicides in beverages and celtuces. High sensitivity was achieved, with method detection limit (S/N = 3) of 0.01–––0.025 ng mL−1 for beverages, 1.70 ng g−1 for celtuce, and quantitation limits of 0.03–––0.10 ng mL−1 for beverages, 5.00 ng g−1 for celtuce. The method recoveries were 80.5–––120.0 % with relative standard deviations lower than 6.1%. Adsorption mechanism mainly involved F-π, F-O, π-π, polar interactions and hydrogen-bonding interactions. This study offers a simple protocol to develop multi-functional sorbents for extraction of organic pollutants." @default.
- W4382583693 created "2023-06-30" @default.
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- W4382583693 date "2023-11-01" @default.
- W4382583693 modified "2023-10-14" @default.
- W4382583693 title "Preparation of hypercrosslinked porous polymer with manifold functional groups for sensitive determination of phenylurea herbicides in beverages and celtuce samples" @default.
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- W4382583693 doi "https://doi.org/10.1016/j.foodchem.2023.136674" @default.
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