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- W4382933650 abstract "Sintering and thermogravimetric experiments, coupled to microstructure investigations and phase structure analyses, were carried out on a homogeneous U0.89Pu0.11O2+x MOX fuel under an atmosphere made of Ar + 4 vpm O2. A significant weight gain (+2.4 wt%, oxidation step) is observed at low temperatures (≤590°C) without any swelling of the pellet. Raman spectroscopy characterizations indicated the presence of the M3O7 phase (M=U/Pu). At higher temperatures (between 1200 and 1540°C), a weight loss (-2.2 wt%, reduction step) is observed. In the same time, swelling of the pellet is detected due mostly to the release of dioxygen from the sample over-oxidized areas, leading ultimately to the typical solarisation microstructure (core/shell structure, large grains in the core and small grains in the shell, residual pores located at multiple grain junctions in both cases). The temperature range 590-1200°C is related mainly to densification and grain growth." @default.
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- W4382933650 date "2023-11-01" @default.
- W4382933650 modified "2023-10-18" @default.
- W4382933650 title "MOX fuel sintering under oxidizing conditions: A comprehensive study of the solarisation phenomenon" @default.
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- W4382933650 doi "https://doi.org/10.1016/j.jeurceramsoc.2023.06.072" @default.
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