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- W4384200904 abstract "Hydrothermal synthesis of molybdenum disulfide (MoS2) with varying S/Mo precursor ratios results in nanoparticle formation with the 2H-crystallographic phase, alongside a significant content of molybdenum reduced oxide (MoO3–x), as confirmed by Raman and X-ray photoelectron spectroscopy (XPS) measurements. Three distinct paramagnetic defect centers are identified by low-temperature electron paramagnetic resonance (EPR) measurements, with the spins localized around sulfur vacancy centers offering the strongest signal. Oxygen vacancies present in the MoO3–x offer the longest spin dephasing time (7.19 μs), whereas the spins localized in Mo-antisites show the fastest spin dephasing. Temperature-dependent resistivity measurements disclose a transition from three-dimensional variable range hopping (3D-VRH) to thermally activated transport (TAT), where the transition temperature (Ttr) correlates with the MoO3–x content and the activation energy of TAT transport correlates to the sample morphology. Energy associated with the 3D-VRH transport, on the other hand, can be correlated with the degree of disorderedness of the samples. Annealing in an inert environment is found to improve the sample crystallinity and enhance the threshold energies of charge transport and homogeneity of the paramagnetic sites." @default.
- W4384200904 created "2023-07-14" @default.
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- W4384200904 date "2023-07-13" @default.
- W4384200904 modified "2023-09-25" @default.
- W4384200904 title "Study of Spin Localization and Charge Transport in Hydrothermally Synthesized 2H-MoS<sub>2</sub>" @default.
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- W4384200904 doi "https://doi.org/10.1021/acs.jpcc.3c02855" @default.
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