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- W4384274030 abstract "A series of hydrazone-based N,O-chelate half-sandwich iridium complexes were synthesized through a facile route with good yields. These air- and moisture-stable iridium complexes exhibited excellent catalytic activity in the cyanosilylether synthesis under mild reaction conditions. Under the catalysis of iridium, various cyanosilylethers with different substituents were obtained through a one-pot reaction of trimethylsilyl cyanide (TMSCN) with carbonyl substrates, with good to excellent yields. The excellent catalytic efficiency, wide substrate range, and mild reaction conditions made this type of iridium catalyst have the potential for industrial applications. All the half-sandwich iridium complexes were well characterized by IR, NMR, and EA analyses. The molecular structure of iridium complex 1 was confirmed by single-crystal X-ray analysis." @default.
- W4384274030 created "2023-07-15" @default.
- W4384274030 creator A5007329641 @default.
- W4384274030 creator A5035459741 @default.
- W4384274030 creator A5039657597 @default.
- W4384274030 creator A5044605728 @default.
- W4384274030 date "2023-01-01" @default.
- W4384274030 modified "2023-10-06" @default.
- W4384274030 title "Half-Sandwich Iridium Complexes with Hydrazone Ligands: Preparation, Structure and Catalytic Synthesis of Cyanosilylethers under Air" @default.
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- W4384274030 doi "https://doi.org/10.1039/d3dt01617j" @default.