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- W4384648453 abstract "Abstract A three-component approach was conducted to adeptly prepare a new series of ( Z )-bis( N -phenylthiazol-2(3 H )-imines. The newly synthesized compounds were prepared by refluxing a ternary mixture of phenyl isothiocyanate, the suitable α-bromoketones, and alkane-linked diamines in ethanol. Reaction conditions were optimized by comparing the yield of the final product under various bases, solvents, temperatures, and base-to-starting-materials molar ratios. The intended hybrids were produced with 85–96% yields while using ethanol at 80 °C for 3–5 h in the presence of anhydrous sodium acetate. The ascribed configuration of new products as well as the regioselectivity of the one-pot reaction were confirmed using both spectral data (1D and 2D NMR) and DFT-calculation techniques. Graphical abstract" @default.
- W4384648453 created "2023-07-19" @default.
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- W4384648453 date "2023-07-19" @default.
- W4384648453 modified "2023-10-14" @default.
- W4384648453 title "Regioselective three-component synthesis and theoretical calculations of new alkane-linked bis(thiazol-2(3H)-imine) hybrids: a DFT-based FMO and local reactivity indices" @default.
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- W4384648453 doi "https://doi.org/10.1007/s13738-023-02851-5" @default.
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