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- W4384666148 abstract "The porous aluminophosphate AlPO4-17 with a hexagonal erionite structure, exhibiting very strong negative thermal expansion, anomalous compressibility, and pressure-induced amorphization, was studied at high pressure by single-crystal and powder X-ray diffraction in the penetrating pressure transmitting media N2, O2, and Ar. Under pressure, these guest species were confirmed to enter the pores of AlPO4-17, thus completely modifying its behavior. Pressure-induced collapse in the xy plane of AlPO4-17 no longer occurred, and this plane exhibited close to zero area compressibility. Pressure-induced amorphization was also suppressed as the elastic instability in the xy plane was removed. Crystal structure refinements at a pressure of 5.5 GPa indicate that up to 28 guest molecules are inserted per unit cell and that this insertion is responsible for the reduced compressibility observed at high pressure. A phase transition to a new hexagonal structure with cell doubling along the a direction was observed above 4.4 GPa in fluid O2." @default.
- W4384666148 created "2023-07-20" @default.
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- W4384666148 date "2023-07-18" @default.
- W4384666148 modified "2023-09-25" @default.
- W4384666148 title "Strongly Modified Mechanical Properties and Phase Transition in AlPO<sub>4</sub>-17 Due to Insertion of Guest Species at High Pressure" @default.
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- W4384666148 doi "https://doi.org/10.1021/acs.jpcc.3c03513" @default.
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