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- W4385330892 abstract "A variety of cyclic alcohols are found to undergo nitrogen insertion by subjection to O-mesitylsulfonylhydroxylamine. Critical to a successful process is the use of fluorinated alcoholic solvents, which ensures sufficient substrate activation to allow engagement with the ambiphilic aminating agent. This transition-metal-free nitrogen insertion provides access to a variety of medicinally relevant heterocycles such as pyrrolidenes, quinolines, and benzazepines (24 examples). Furthermore, combination with a photochemical Norrish-Yang-type cyclization allows an unprecedented access to indoles from ortho-substituted acetophenones." @default.
- W4385330892 created "2023-07-29" @default.
- W4385330892 creator A5003385047 @default.
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- W4385330892 date "2023-07-28" @default.
- W4385330892 modified "2023-10-17" @default.
- W4385330892 title "From Cycloalkanols to Heterocycles via Nitrogen Insertion" @default.
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- W4385330892 doi "https://doi.org/10.1021/acs.orglett.3c02048" @default.
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