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• W4385374321 abstract "A Cu-electrocatalytic azidation of N-aryl enamines and subsequent denitrogenative annulation for the construction of quinoxaline frameworks is reported. Only 0.5 mol % of copper(II) chloride was employed for this cascade transformation displaying excellent functional-group compatibility even with complex bioactive scaffolds. The efficient electro-oxidative protocol enables the use of NaN3 as the cheapest azide source. Detailed mechanistic experiments, cyclic voltammetry, and spectroscopic studies provided strong evidence for a dual role of the Cu catalyst in azidyl and iminyl radical generation steps." @default.
• W4385374321 created "2023-07-29" @default.
• W4385374321 creator A5022608287 @default.
• W4385374321 creator A5030434402 @default.
• W4385374321 date "2023-07-29" @default.
• W4385374321 modified "2023-10-17" @default.
• W4385374321 title "Synthesis of Quinoxalines through Cu-electrocatalytic Azidation/Annulation Cascade at Low Catalyst Loading" @default.
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• W4385374321 doi "https://doi.org/10.1021/acs.orglett.3c02186" @default.
• W4385374321 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/37515784" @default.
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