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• W4385442600 abstract "Dynamic nuclear polarization (DNP) is routinely used as a method for increasing the sensitivity to nuclear magnetic resonance (NMR). Recently, high-field solid-effect DNP in viscous liquids on 1H nuclei was demonstrated using narrow-line polarizing agents. Here we expand the applicability of DNP in viscous media to 13C nuclei. To hyperpolarize 13C nuclei, we combined solid-effect 1H DNP with a subsequent transfer of the 1H polarization to 13C via insensitive nuclei enhanced by polarization transfer (INEPT). We demonstrate this approach using a triarylmethyl radical as a polarizing agent and glycerol-13C3 as an analyte. We achieved 13C enhancement factors of up to 45 at a magnetic field of 9.4 T and room temperature." @default.
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• W4385442600 date "2023-08-01" @default.
• W4385442600 modified "2023-09-27" @default.
• W4385442600 title "¹³C Hyperpolarization of Viscous Liquids by Transfer of Solid-Effect ¹H Dynamic Nuclear Polarization at High Magnetic Field" @default.
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• W4385442600 doi "https://doi.org/10.1021/acs.jpclett.3c01732" @default.
• W4385442600 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/37526333" @default.
• W4385442600 hasPublicationYear "2023" @default.
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