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- W4385486822 abstract "Multi-anvil press (MAP) is a major type of apparatus for phase equilibrium, material synthesis, and property investigations at up to 120 GPa of static compression. Here I summarize the fundamental aspects of the MAP techniques, highlighting uncertainties in pressure and temperature in experiments using tungsten carbide (WC) anvils with 3 mm and 5 mm truncation edge lengths (TEL). To illustrate the application of the MAP for synthesizing millimeter-sized single crystals of deep mantle silicates, I review the theory of crystal growth and compile relevant phase diagrams. The theory informs synthesis methods such as slow cooling of a fluid solution and growing crystals in a thermal gradient. The updated phase diagrams involve Mg2SiO4, MgSiO3, and H2O at pressures up to 27 GPa and touch upon iron-bearing compositions. Also reviewed briefly are techniques to characterize the compositions and structures of synthesis products." @default.
- W4385486822 created "2023-08-03" @default.
- W4385486822 creator A5085352453 @default.
- W4385486822 date "2022-11-24" @default.
- W4385486822 modified "2023-10-16" @default.
- W4385486822 title "Synthesis of High-Pressure Silicate Polymorphs Using Multi-Anvil Press" @default.
- W4385486822 doi "https://doi.org/10.1017/9781108806145.012" @default.
- W4385486822 hasPublicationYear "2022" @default.
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