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- W4385514812 abstract "Abstract This article reviews the analytical tool chest used for characterizing alkoxylates and their associated copolymer mixtures. Specific emphasis will be placed upon the use of mass spectrometry‐based techniques as rapid characterization tools for optimizing reaction processes in an industrial R&D setting. An initial tutorial will cover the use of matrix‐assisted laser desorption/ionization‐mass spectrometry and tandem mass spectrometry fragmentation for detailed component analysis (e.g., polyol and isocyanate) of a model polyurethane‐based foam. Next, this critical feedback information will be used with the guidance of mass spectrometry to initiate the development of a new, more efficient, tris(pentafluorophenyl)borane (FAB) catalyst‐based alkoxylation process for generating the next generation of glycerin‐initiated poly(propylene oxide)‐ co ‐poly(ethylene oxide) copolymers. Examples will be provided for each step in the FAB‐based optimization process that were required to generate the final product. Following this example, two‐dimensional liquid chromatography, supercritical fluid chromatography, and ion mobility separations, along with their coupling to mass spectrometry, will be reviewed for their efficiency in characterizing and quantitating the components within these complex polyether polyol mixtures." @default.
- W4385514812 created "2023-08-04" @default.
- W4385514812 creator A5000691058 @default.
- W4385514812 creator A5012749450 @default.
- W4385514812 creator A5014852078 @default.
- W4385514812 creator A5023324383 @default.
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- W4385514812 creator A5047075291 @default.
- W4385514812 creator A5070161759 @default.
- W4385514812 creator A5088283556 @default.
- W4385514812 date "2023-08-03" @default.
- W4385514812 modified "2023-09-27" @default.
- W4385514812 title "Microstructure characterization and mechanistic insight into polyether polyols and their associated polyurethanes" @default.
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