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- W4385545488 abstract "As the ongoing research in cation-conductive thiophosphates attracted attention especially for the Li+-ion conducting materials, their great structural variety and potential application motivated research on other thiophosphates as well. Here we present the silver-containing yttrium thiophosphate(V) Ag3Y[PS4]2 (a = 1697.65(9), b = 924.38(5), c = 937.46(5) pm, β = 123.217(3)°, Z = 4) plus three new lanthanoid representatives, namely Ag3Dy[PS4]2, Ag3Ho[PS4]2 and Ag3Er[PS4]2, crystallizing isotypically in the monoclinic space group C2/c. These new compounds were synthesized from the respective sulfides (Ag2S, RE2S3 and P2S5; RE = Y, Dy, Ho and Er) in fused glassy silica ampoules under inert conditions at 700 °C. The crystal structure of the materials was revisited to reveal [AgS4]7–, [RES8]13− and [PS4]3– polyhedra as building blocks, and spectroscopic studies were first performed on these particular Ag3RE[PS4]2 samples. Electrochemical impedance spectroscopy (EIS) shed light on the Ag+-conducting potential of these thiophosphates for the example of Ag3Ho[PS4]2. Raman-spectroscopic investigations confirmed the presence of [AgS4]7– and discrete [PS4]3– tetrahedra and the studies of the diffuse reflectance (DRS) revealed optical band gaps of Eg = 2.4–2.7 eV." @default.
- W4385545488 created "2023-08-04" @default.
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- W4385545488 date "2023-09-01" @default.
- W4385545488 modified "2023-09-23" @default.
- W4385545488 title "Structure, spectroscopic investigations and discussion on conductivity of rare-earth metal thiophosphates(V) hosting silver ions in the Ag3RE[PS4]2 series (RE = Y, Dy, Ho and Er)" @default.
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- W4385545488 doi "https://doi.org/10.1016/j.solidstatesciences.2023.107280" @default.
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