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• W4385564688 endingPage "11884" @default.
• W4385564688 startingPage "11874" @default.
• W4385564688 abstract "A direct arylsulfonylation of β,γ-unsaturated hydrazones method, in which sulfonated pyrazolines are accessed by a three-component reaction of β,γ-unsaturated hydrazones, DABSO, and aryldiazonium tetrafluoroborates, has been developed without external oxidants or catalysts. This transformation is triggered by the formation of arylsulfonyl radicals in situ from the reaction of aryldiazonium tetrafluoroborates and DABSO, and is enabled by controllable generation of C center radical, in which DABSO was utilized as the sulfone source and an oxidant in this radical-mediated cascaded reaction. A wide range of substrates can be applied in this process to afford pyrazolines in good yield, and it is amenable for gram-scale synthesis." @default.
• W4385564688 created "2023-08-05" @default.
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• W4385564688 date "2023-08-03" @default.
• W4385564688 modified "2023-10-14" @default.
• W4385564688 title "Annulative Aminosulfonylation of Unactivated Alkenes for Accessing Pyrazolines via Multicomponent SO₂ Insertion" @default.
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• W4385564688 doi "https://doi.org/10.1021/acs.joc.3c01163" @default.
• W4385564688 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/37535756" @default.
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