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• W4385655691 abstract "The elaboration of step-economy and catalytic approaches for accessing diverse fluorinated heterocyclics is highly desirable. Described herein is a radical-polar crossover enabled three-component cyclization to polysubstituted fluoropyrazoles by using CF2Br2 as a novel C1F1 synthon. Mechanistic experiments revealed that the in situ generation of the reactive intermediate gem-difluorovinylimine ion is the key to this transformation. This protocol unlocks the novel reactivity of CF2Br2 and adds significant synthetic values to fluorine chemistry." @default.
• W4385655691 created "2023-08-09" @default.
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• W4385655691 date "2023-08-08" @default.
• W4385655691 modified "2023-09-25" @default.
• W4385655691 title "Radical-Polar Crossover Enabled Triple Cleavage of CF₂Br₂: A Multicomponent Tandem Cyclization to 3-Fluoropyrazoles" @default.
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• W4385655691 doi "https://doi.org/10.1021/acs.orglett.3c02305" @default.
• W4385655691 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/37552672" @default.
• W4385655691 hasPublicationYear "2023" @default.
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