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- W4385879657 abstract "Herein, a selective synthesis of isocoumarin and 3-benzylidenaphthalides via Heck-type ortho-olefination of benzoic acids with vinyl arenes is reported under the mild reaction protocols. The present reaction was catalyzed by a well-established selenated NHC-Pd(II) pincer complex and Ag(OAc) as an oxidant. All reactions works in water, which is a green eco-friendly solvent; moreover, the method's effectiveness is highlighted by the selective synthesis of isocoumarin or 3-benzylidenaphthalides in moderate to good yield. The functional group associated with benzoic acids and vinyl arenes did not exhibit any detrimental effect and displayed the protocol's efficacy. In a nutshell, the present method of oxidative coupling of benzoic acid and vinylarenes entail a lower amount of catalyst and oxidant loading, works effectively with green solvent water, and produces the selective isocoumarin product in 12-14 hours under aerobic conditions." @default.
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- W4385879657 date "2023-11-01" @default.
- W4385879657 modified "2023-10-17" @default.
- W4385879657 title "Water mediated NHC-Pd (II) catalyzed oxidative coupling of benzoic acid and vinylarenes; Selective synthesis of five/six member isocoumarins" @default.
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- W4385879657 doi "https://doi.org/10.1016/j.jorganchem.2023.122847" @default.
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