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- W4386200410 abstract "Laser-heated melts based on the 43CaO–57Fe 2 O 3− x eutectic, close to the calcium ferrite (CF) composition, were measured with high-energy X-ray diffraction using aerodynamic levitation over a range of redox states controlled by CO/CO 2 gas atmospheres. The iron–oxygen coordination number was found to rise from 4.4 ± 0.3 at 15% Fe 3+ to 5.3 ± 0.3 at 87% Fe 3+ . Empirical potential structure refinement modelling was used to obtain the ferric and ferrous partial pair distribution functions. It was found that the Fe 2+ iron–oxygen coordination number is consistently approximately 10% higher in CF than in pure iron oxide, while Fe 3+ is essentially identical in all but the most oxygen-rich environments (where it is higher in CF compared with FeO x ). The model also shows calcium octahedra to be the dominant species across all redox environments, although the population of CaO 7 increases with the availability of oxygen at the expense of CaO 4 and CaO 5 . This article is part of the theme issue ‘Exploring the length scales, timescales and chemistry of challenging materials (Part 1)’." @default.
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- W4386200410 date "2023-08-28" @default.
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- W4386200410 title "The structure of molten calcium ferrite under various redox conditions" @default.
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- W4386200410 doi "https://doi.org/10.1098/rsta.2022.0352" @default.
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