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• W4386442822 abstract "In this work, an in-situ Al 3 Ti–Al 2 O 3 composite was optimally synthesized from raw powders via mechanical milling and conventional sintering processes. The strong influence of milling time on the promotion of the phase reaction between the initial TiO 2 and Al materials was proven by using X-ray diffraction and surface morphology analysis. The obtained results showed that the milling process did not initiate any reaction between the raw TiO 2 and Al materials. However, the milling process was important for creating a homogeneous powder mixture and refining the particle size of the powders. The Al 3 Ti–Al 2 O 3 composites were completely formed after conventional sintering at 750°C for 30 min for a milling time of over 4 h. The highest obtained microhardness of the composite was approximately 130 HV, which was suggested to be related to the microstructure of the bulk composite specimen consisting of two main phases, the Al 3 Ti matrix and the Al 2 O 3 particles dispersed in the matrix. A small portion of an unidentified phase, a Ti-rich compound, was found in the matrix together with a tiny fraction of AlTi 3 . We suggest that the optimal sintering process and mechanical milling are important key factors in fabricating bulk hardness Al 3 Ti–Al 2 O 3 composite materials." @default.
• W4386442822 created "2023-09-06" @default.
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• W4386442822 date "2023-09-05" @default.
• W4386442822 modified "2023-09-26" @default.
• W4386442822 title "Fabrication and hardness of in-situ Al3Ti–Al2O3 composite" @default.
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• W4386442822 doi "https://doi.org/10.3389/fmats.2023.1265903" @default.
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