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- W4386467524 abstract "Arylglycines are important pharmacophores present in several top-selling drugs. This compound class has now been made accessible from abundant aryl chlorides by a Pd-catalyzed Schöllkopf-type amino acid synthesis. In the presence of the catalyst methylnaphthyl(XPhos)-palladium bromide, the base lithium 2,2,6,6-tetramethylpyrrolidide and the additive ZnCl2 , tert-leucine-derived bis-lactim ethers were efficiently arylated at room temperature, reaching yields of 95 % and diastereoselectivities of 98 : 2. Hydrolysis gave the corresponding arylglycines in high enantiomeric excess." @default.
- W4386467524 created "2023-09-07" @default.
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- W4386467524 date "2023-09-26" @default.
- W4386467524 modified "2023-10-16" @default.
- W4386467524 title "Enantioselective Synthesis of Arylglycines via Pd‐Catalyzed Coupling of Schöllkopf Bis‐Lactim Ethers with Aryl Chlorides" @default.
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- W4386467524 doi "https://doi.org/10.1002/anie.202309868" @default.
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