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- W4386573886 abstract "In this work, sixteen deep eutectic solvents and four conventional solvents were tested for polysaccharide and antioxidant extraction from Persian manna (Taranjabin). Choline chloride-xylitol was selected as the best solvent. Extraction variables such as temperature (T), time (t), water content in DES (WC), and liquid-to-solid ratio (L/s) in ultrasonic-assisted extraction were optimized by the Box-Behnken design and response surface methodology (RSM). At optimal conditions (T = 70 ◦C, WC = 10% v/v, L/s ratio = 100 mL/g and t = 40 min), total carbohydrate content and extraction yield were 2.5 mg Glu per gram of dried and deffated material (gddm) and 55.5%, respectively. Based on monosaccharide composition analysis, extracted polysaccharides had rhamnose, arabinose, glucose and galactose (molar ratio: 1.68:0.69:1.00:2.16). Different antioxidant assays such as total phenolic and total flavonoid content, DPPH assay, trolox equivalent antioxidant capacity, ferric-reducing antioxidant power and reducing power assay were also performed. Optimal extraction conditions for total phenolic content were T = 70 ◦C, WC = 50% v/v, L/s ratio = 100 mL/g and t = 20 min. Experimental TPC was 2.15 mg GAE/gddm. Extraction efficiencies of the DES-based ultrasonic-assisted method for total carbohydrates and phenolics contents (2.50 mg Glu/gddm and 2.15 mg GAE/gddm) were better than microwave-assisted extraction (1.03, 1.15), maceration (0.64, 0.72) and Soxhlet methods (1.13, 0.88). In comparison of DES and water in ultrasonic-assisted extraction, extraction improvement for DES (choline chloride-xylitol) was about 26% in TCC (1.057 vs. 0.839 mg Glu/gddm), and 56% in TPC (0.528 vs. 0.339 mg GAE/gddm) with respect to water." @default.
- W4386573886 created "2023-09-10" @default.
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- W4386573886 date "2023-11-01" @default.
- W4386573886 modified "2023-09-27" @default.
- W4386573886 title "Deep eutectic solvent mediated extraction of polysaccharides and antioxidants from Persian manna (Taranjabin): Comparison of different extraction methods and optimization by response surface methodology" @default.
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- W4386573886 doi "https://doi.org/10.1016/j.microc.2023.109336" @default.
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