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• W4386593353 abstract "1,2,6-Thiadiazines treated with visible light and 3O2 under ambient conditions are converted into difficult-to-access 1,2,5-thiadiazole 1-oxides (35 examples, yields of 39–100%). Experimental and theoretical studies reveal that 1,2,6-thiadiazines act as triplet photosensitizers that produce 1O2 and then undergo a chemoselective [3 + 2] cycloaddition to give an endoperoxide that ring contracts with selective carbon atom excision and complete atom economy. The reaction was optimized under both batch and continuous-flow conditions and is also efficient in green solvents." @default.
• W4386593353 created "2023-09-12" @default.
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• W4386593353 date "2023-09-11" @default.
• W4386593353 modified "2023-10-17" @default.
• W4386593353 title "The Photochemical Mediated Ring Contraction of 4<i>H</i>-1,2,6-Thiadiazines To Afford 1,2,5-Thiadiazol-3(2<i>H</i>)-one 1-Oxides" @default.
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• W4386593353 doi "https://doi.org/10.1021/acs.orglett.3c02673" @default.
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