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• W4386885503 startingPage "108942" @default.
• W4386885503 abstract "Base-promoted (MeONa in MeOH or imidazole in DMF) isomerization of a series of 3,4,6-tri-O-benzyl-d-gluco- and d-mannopyranose derivatives with triisopropylsilyl (TIPS) substituents was studied. The presence of a bulky TIPS group at O-1 or O-2 was shown to be favorable for the isomerization of benzyl protected d-gluco- and d-mannopyranose derivatives to d-fructofuranose derivatives, in which the bulky silyl group occupies less sterically hindered primary position. The highest yield (33%) of the fructofuranose derivative was achieved when 3,4,6-tri-O-benzyl-2-O-triisopropylsilyl-d-mannopyranose was treated with MeONa in MeON at 50 °C." @default.
• W4386885503 created "2023-09-21" @default.
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• W4386885503 date "2023-12-01" @default.
• W4386885503 modified "2023-09-30" @default.
• W4386885503 title "TIPS group-assisted isomerization of benzyl protected d-manno- and d-glucopyranose to d-fructofuranose derivatives" @default.
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• W4386885503 doi "https://doi.org/10.1016/j.carres.2023.108942" @default.
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