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- W4386915212 abstract "Abstract This article reports, for the first time, the experimental in-situ three-dimensional measurements of the E -field’s uniform distribution of Variable Frequency Microwaves (VFM) within a multimode cavity under high power conditions, and subsequent comparison to fixed frequency microwaves (FFM). Such distribution could earlier be assessed only through a theoretical analysis. The article also examines the consequences of changes in VFM irradiation conditions and elucidates the threshold at which VFM irradiation is beneficial. With an ultimate focus of the use of VFM microwave radiation toward industrial applications, the effective synthesis of 4-methylbyphenyl (4-MBP) carried out in the presence of Pd (catalyst) supported on activated carbon particulates (Pd/AC) was revisited with two principal objectives:(a) the effective suppression of discharge phenomena (formation of hot spots); and (b) the scale-up of the synthesis using a 5-fold increase in sample quantity and a 7.5-fold larger reactor size (diameter) than used in earlier studies." @default.
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- W4386915212 date "2023-09-21" @default.
- W4386915212 modified "2023-10-16" @default.
- W4386915212 title "Three-Dimensional Observations of the Electric Field Distribution of Variable Frequency Microwaves: Scaling-up Organic Syntheses" @default.
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- W4386915212 doi "https://doi.org/10.21203/rs.3.rs-3324583/v1" @default.
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