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- W4386945597 abstract "In this work, eight compounds from Phellodendron chinense were separated and purified by pH-zone refining counter-current chromatography and traditional counter-current chromatography coupled with online-storage inner-recycling counter-current chromatography (IRCCC). The pH-zone-refining mode was adopted for separating 2.0 g of crude extract with the solvent system of chloroform-methanol-water (4:3:3, v/v), in which 10 mM hydrochloric acid and 10 mM triethylamine were added in the stationary and mobile phases, respectively. Meanwhile, traditional counter-current chromatography coupled with online-storage IRCCC separation was performed by the solvent system of n-hexane-ethyl acetate-methanol-water (5:5:2:8, v/v). Finally, eight compounds, including six alkaloids as 6-methylpiperidin-2-one(1), isoplatydesmine(4), berlambine(5), epiberberine(6), palmatine(7), berberine(8) and two phenolic acids as ferulic acid(2), isoferulic acid(3), were successfully obtained using these three different CCC modes with the purities over 95.0%." @default.
- W4386945597 created "2023-09-23" @default.
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- W4386945597 date "2023-09-22" @default.
- W4386945597 modified "2023-10-12" @default.
- W4386945597 title "Separation and purification of alkaloids and phenolic acids from <i>Phellodendron chinense</i> by pH‐zone refining and online‐storage inner‐recycling counter‐current chromatography" @default.
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- W4386945597 doi "https://doi.org/10.1002/jssc.202300497" @default.
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