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- W4387071805 abstract "Homoallenic alcohols are versatile building blocks to access complex molecules in synthetic chemistry. We present a protocol for accessing homoallenic alcohols by an allenyl radical-involved radical-polar crossover process. We describe steps for preparing solvents and the photoreactor and synthesizing 5-methyl-1-phenyl-3-tosylhexa-3,4-dien-1-ol 3 in 85% yield. In addition, 5-methyl-1-phenyl-3-tosylhexa-3,4-dien-1-ol 3 has been successfully synthesized in 2-mmol scale. This protocol is also applicable to the synthesis of homoallenic amides. For complete details on the use and execution of this protocol, please refer to Wei et al. (2023).1" @default.
- W4387071805 created "2023-09-27" @default.
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- W4387071805 date "2023-12-01" @default.
- W4387071805 modified "2023-10-09" @default.
- W4387071805 title "Protocol for the synthesis of homoallenic alcohols via allenyl radical-mediated allenylation of alkenes" @default.
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- W4387071805 doi "https://doi.org/10.1016/j.xpro.2023.102598" @default.
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