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- W4387307612 abstract "Abstract By exploiting coordination‐driven self‐assembly, high yields of two 8 18 molecular metalla‐knots could be obtained using a thiazole‐moiety‐containing asymmetric dipyridyl ligand 2‐(pyridin‐4‐yl)‐5‐(pyridin‐4‐ylethynyl)benzo[ d ]thiazole ( L 1 ), as confirmed using X‐ray crystallographic analysis, electrospray ionization‐time‐of‐flight/mass spectrometry (ESI‐TOF/MS), and detailed liquid‐state nuclear magnetic resonance (NMR) spectroscopy. To modulate the self‐assembled structures, m ‐chloroperbenzoic acid ( m ‐CPBA) was utilized to oxidize thiazole‐based ligand L 1 to N‐thiazole‐oxide‐based ligand 2‐(pyridin‐4‐yl)‐5‐(pyridin‐4‐ylethynyl)benzo[d]thiazole 3‐oxide ( L 2 ), which enabled the selective construction of the corresponding tetranuclear macrocycles. Notably, two molecular metalla‐knots could be topologically transformed from 8 18 knots to simple monocycles because the L 1 alkyne bond was inert toward m ‐CPBA, as confirmed by liquid‐state NMR spectroscopy, ESI‐TOF/MS, and elemental analysis." @default.
- W4387307612 created "2023-10-04" @default.
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- W4387307612 date "2023-10-13" @default.
- W4387307612 modified "2023-10-15" @default.
- W4387307612 title "Controllable Topological Transformations of 818 Molecular Metalla‐knots via Oxidation of Thiazole‐based Ligands" @default.
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- W4387307612 doi "https://doi.org/10.1002/ange.202313605" @default.
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