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- W4387328237 abstract "Dual functionalization in organic synthesis is an elegant and powerful method for simultaneously introducing two different functional groups regio-selectively into a target molecule. We herein describe our recent work on retained dual functionalization and dehydrogenative dual functionalization via oxidation of halogen. For the dehydrogenative dual functionalization by oxidation of bromide ion, a catalytic dual functionalization of ethers through dealkylation-oxidation-bromination accompanied by C-O bond cleavage via aerobic oxidation of bromide was developed to obtain α-bromo ketones. Furthermore, a nitrite-catalyzed ring-contraction reaction of substituted tetrahydropyrans by oxidation of bromide under aerobic conditions was discovered to provide 2-acyltetrahydrofurans. We also succeeded a regio-selective Csp2-Csp2 bromo-amination of indole derivatives via the 1,3-migration of imides on indolyl(phenyl)iodonium imides and a remote Csp2-Csp3 iodo-amination of 2-methyl indole derivatives with iodinating reagents to furnish the corresponding halo-amino-indole derivatives via formation of indolyl(phenyl)iodonium imides from indole derivatives, bis(sulfonyl)imides, and (diacetoxy)iodobenzene as the retained dual functionalization using hypervalent iodine (III)." @default.
- W4387328237 created "2023-10-05" @default.
- W4387328237 creator A5078415532 @default.
- W4387328237 date "2023-10-01" @default.
- W4387328237 modified "2023-10-09" @default.
- W4387328237 title "Dual Functionalization of Organic Compounds via Oxidation of Halogen" @default.
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- W4387328237 doi "https://doi.org/10.5059/yukigoseikyokaishi.81.951" @default.
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