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- W4387409675 abstract "AbstractA greener and direct approach to the efficient synthesis of fused heterocyclic ring system benzo[4,5]imidazo[2,1-b]thiazoles via C–N and C–S bond formation in catalyst-free conditions has been reported using 2,2,2-trifluoroethanol (TFE) as a reaction medium at room temperature. The salient features of this approach include an elementary and clean reaction protocol to afford the desired product in higher yields in less reaction time with sufficient purity. This prominent moiety is frequently found in many natural bioactive occurring compounds and shows potential in synthesizing diverse biologically active compounds due to their therapeutic values. The synthesis of benzo[4,5]imidazo[2,1-b]thiazoles was confirmed by spectral analysis and also by DFT studies.KEYWORDS: Benzo[4,5]imidazo[2,1-b]thiazole; catalyst-free2,2,2-trifluoroethanolDFT studiesgreener approach AcknowledgementsAuthors thank DST, New Delhi, for a start-up grant (SERB). We thank Malaviya National Institute of Technology (MNIT) Jaipur and Central Drug Research Institute (CDRI), Lucknow, for the spectral and elemental analysis.Disclosure statementNo potential conflict of interest was reported by the author(s).Additional informationFundingThis work was supported by SERB [grant number YSS/2015/000972]." @default.
- W4387409675 created "2023-10-07" @default.
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- W4387409675 date "2023-10-06" @default.
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- W4387409675 title "Computational and experimental analysis of catalyst-free and expeditious synthesis of Benzo[4,5]imidazo[2,1- <i>b</i> ]thiazole derivatives" @default.
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- W4387409675 doi "https://doi.org/10.1080/17415993.2023.2266083" @default.
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