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• W4387566262 endingPage "132776" @default.
• W4387566262 startingPage "132776" @default.
• W4387566262 abstract "Magnetic solid-phase extraction (MSPE) was developed based on a well-designed Fe3O4-NH2 @g-C3N4 nanocomposite as sorbent for a mixture of six benzophenones (BPs) in environmental water samples. The composite fabricated via in-situ self-assembled g-C3N4 shell with homogeneous polymerization of cyanuric chloride and cyanuric acid on Fe3O4-NH2 core. While high adsorption capacity was derived from g-C3N4 via hydrophobic, π-π and hydrogen bonding interactions to the targets, the fast magnetic separation was realized with Fe3O4 core for less solvent consumption. In combination with LC-MS/MS, the Fe3O4-NH2 @g-C3N4 sorbent minimized the interfering components, reduced the matrix effects, and provided the enrichment factors of 121-150 for six BPs with relative standard deviations ≤ 9.7% even after 20 times extraction-desorption cycles. The present method gave the detection limits of 0.3-2.5 ng/L for six BPs with the linear ranges of 1.0-2000 ng/L, and the recoveries of 84.6%-104% in sea water and 86.2%-107% in lake water samples. Thus, the Fe3O4-NH2 @g-C3N4-based MSPE coupled with LC-MS/MS method provided a convenient, efficient, and reliable alternative to monitor trace BPs in environmental water samples." @default.
• W4387566262 created "2023-10-13" @default.
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• W4387566262 date "2024-01-01" @default.
• W4387566262 modified "2023-10-18" @default.
• W4387566262 title "Self-assembled Fe3O4-NH2@g-C3N4 composite for magnetic solid-phase extraction of benzophenones in sea water and lake water coupled with LC-MS/MS determination" @default.
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• W4387566262 doi "https://doi.org/10.1016/j.jhazmat.2023.132776" @default.
• W4387566262 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/37844496" @default.
• W4387566262 hasPublicationYear "2024" @default.
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